Blank corrections for ramped pyrolysis radiocarbon dating of sedimentary and soil organic carbon

Long, R. High sensitivity radiocarbon dating in the 50, to 70, BP range without isotopic enrichment. T1 – High sensitivity radiocarbon dating in the 50, to 70, BP range without isotopic enrichment. N2 – Calculations show the possibility of detecting C remaining after 10 or 11 decay half-lives in natural materials, such as wood, using commercially available liquid scintillation LS detectors. Assuming in-situ C production has contributed insignificantly to the measured C, one can calculate finite ages approaching 70 ka. In practice, defensible finite age determinations involve careful considerations of several critical elements in the procedure. These critical elements are: 1 the integrity of the sample itself, in terms of younger contaminants and of in situ-produced C; 2 the availability of ”dead” background material; 3 chemical blank in laboratory preparation of, in this case, benzene; and 4 stability of background and efficiency of the LS counting system. High-sensitivity C dating reveals a low level of memory effect C in benzene synthesized in the laboratory from anthracite or marble. This level of C activity is equivalent to that found in 53 ka old wood, and thus, is not distinguishable from petrochemical benzene used in routine dating.

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U-Pb dating by zircon dissolution method using chemical abrasion. Nine Temora II zircon grains were analyzed by the laser ablation method yielding an age of Zircon grains of a same population were separated for chemical abrasion before dissolution and mass spectrometry analyses. The age determinations of geological events are a significant tool in basic and applied earth science studies. The complexity of geological processes registered in the minerals can be dated with these techniques.

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Ramped pyrolysis RP targets distinct components of soil and sedimentary organic carbon based on their thermochemical stabilities and allows the determination of the full spectrum of radiocarbon 14 C ages present in a soil or sediment sample. Extending the method into realms where more precise ages are needed or where smaller samples need to be measured involves better understanding of the blank contamination associated with the method. Here, we use a compiled data set of RP measurements of samples of known age to evaluate the mass of the carbon blank and its associated 14 C signature, and to assess the performance of the RP system.

We estimate blank contamination during RP using two methods, the modern-dead and the isotope dilution method. Our results indicate that during one complete RP run samples are contaminated by 8.

Ramped pyrolysis (RP) targets distinct components of soil and sedimentary organic carbon based on their thermochemical stabilities and.

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Blank corrections for ramped pyrolysis radiocarbon dating of sedimentary and soil organic carbon.

Either your web browser doesn’t support Javascript or it is currently turned off. In the latter case, please turn on Javascript support in your web browser and reload this page. Read article at publisher’s site DOI : Environ Pollut , , 16 Feb Cited by: 13 articles PMID: To arrive at the top five similar articles we use a word-weighted algorithm to compare words from the Title and Abstract of each citation.

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Clicking on the donut icon will load a page at altmetric. Find more information on the Altmetric Attention Score and how the score is calculated. Ramped pyrolysis RP targets distinct components of soil and sedimentary organic carbon based on their thermochemical stabilities and allows the determination of the full spectrum of radiocarbon 14 C ages present in a soil or sediment sample. Extending the method into realms where more precise ages are needed or where smaller samples need to be measured involves better understanding of the blank contamination associated with the method.

Here, we use a compiled data set of RP measurements of samples of known age to evaluate the mass of the carbon blank and its associated 14 C signature, and to assess the performance of the RP system. We estimate blank contamination during RP using two methods, the modern-dead and the isotope dilution method.

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